反应详情

温度

0 °C

A solution of 260 ul of 3-chlorobenzyl alcohol dissolved in 2.5 ml of dry tetrahydrofuran is cooled to 0° C. and 120 ul of PBr3 added. The reaction is stirred for 3 hours and extracted with ether. The organic layer is washed with saturated sodium bicarbonate and evaporated to give the desired product.

1. extractionextracted with ether
2. washThe organic layer is washed with saturated sodium bicarbonate
3. customevaporated