HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha-(4-Methoxycarbonylbenzyloxy)styrene → alpha-[4-(Hydroxymethyl)benzyloxy]styrene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha-(4-Methoxycarbonylbenzyloxy)styrene | HCID 15219435 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | alpha-[4-(Hydroxymethyl)benzyloxy]styrene | HCID 21253606 | — |
Reaction Steps
This compound was prepared by lithium aluminium hydride reduction of α-(4-methoxycarbonylbenzyloxy)styrene: 1H NMR (CCl4) δ 2.65 (1H, t, J 4.5 Hz), 4.15 (1H, d, J 3 Hz), 4.43 (2H, d, J 4.5 Hz), 4.60 (1H, d, J 3 Hz), 4.80 (2H, s), 7.1-7.7 (9H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05874511 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-69887bf1f2cd47b497536a184270d04c |
| Source note | uspto-grants-1999_02 |