HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 363846Generated: October 30, 2026
Dimethylformamide → Homophthalic anhydride
https://huagongshe.com/reaction/363846
Participants
| Role | Name | HCID | Charge |
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| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Product | Homophthalic anhydride | HCID 12801 | — |
Reaction Steps
A solution of homophthalic anhydride (324 mg, 2 mmoles) and triethylamine (0.021 ml, 0.15 mmoles) is prepared in DMF (5 ml) and added to each packet. After heating at 80° C. for 16 hrs the packets are then washed with DMF (3×30 ml) and DCM (3×30 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05874443 |
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| Source dataset | uspto-grants-1999_02 |
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| ORD ID | ord-42abb9285d244a48863da54a5669d20a |
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| Source note | uspto-grants-1999_02 |
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