HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20239949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Methacrylonitrile | HCID 31368 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20239949 | HCID 20239949 | 87.9% |
Reaction Steps
Following the general procedure of Example I, 364 mmols of methacrylonitrile were reacted with 25 mmols of distilled aniline in 30 mL of acetonitrile and in the presence of 38 mmols of concentrated HCl and 2.5 mmols of cuprous oxide. The process resulted in an 87.9% yield of 2-chloro-2-methyl-3-phenylpropionitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04604243 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-56859a13ca184a808ac73b559244948d |
| Source note | uspto-grants-1986_08 |