HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → (2-Chloro-2-phenylethyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Styrene | HCID 7501 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | (2-Chloro-2-phenylethyl)benzene | HCID 20838 | 66.7% |
Reaction Steps
Following the general procedure of Example I, 236 mmols of distilled styrene were reacted with 25 mmols of distilled aniline in 30 mL of acetonitrile and in the presence of 38 mmols of concentrated HCl and 2.5 mmols of cuprous oxide. The process resulted in a 66.7% yield of 2-chloro-1,2-diphenylethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04604243 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-d3ce35c9bc77492786108201bebe8de5 |
| Source note | uspto-grants-1986_08 |