Hydrochloric Acid → 4714-14-1

HRID 363999Notes

Reaction equation

HRID 363999 reaction equation
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.N[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.[ClH:16]>C(#N)C>[Cl:16][CH:1]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 6115AnilineHCID 7501Styrene

Product 1

HCID 208384714-14-1Yield 66.7%

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

Following the general procedure of Example I, 236 mmols of distilled styrene were reacted with 25 mmols of distilled aniline in 30 mL of acetonitrile and in the presence of 38 mmols of concentrated HCl and 2.5 mmols of cuprous oxide. The process resulted in a 66.7% yield of 2-chloro-1,2-diphenylethane.

Sources & evidence

ORD record
ord-d3ce35c9bc77492786108201bebe8de5
Source dataset
uspto-grants-1986_08
Patent number
US04604243

Reaction notes

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