HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20239948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | 3,4-Dimethoxyaniline | HCID 22770 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20239948 | HCID 20239948 | 39.2% |
Reaction Steps
Following the general procedure of Example I, 280 mmols of distilled methyl methacrylate were reacted with 25 mmols of 3,4-dimethoxyaniline in 30 mL of acetonitrile and in the presence of 42 mmols of concentrated HCl and 2.5 mmols of cuprous oxide. The process resulted in a 39.2% yield of methyl 2-chloro-2-methyl-3-(3,4-dimethoxyphenyl)propionate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04604243 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-efa4177446c44d5b9c59dcbc4ffd0314 |
| Source note | uspto-grants-1986_08 |