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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 364076Generated: October 26, 2026

7,8-Dimethoxy-3-[3-(methylamino)propyl]-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one → N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-[3-(3,4-dimethoxyphenylthio)propyl]-methylamine

https://huagongshe.com/reaction/364076

Reaction equation

Participants

RoleNameHCIDCharge
Reactant7,8-Dimethoxy-3-[3-(methylamino)propyl]-1,3,4,5-tetrahydro-2H-3-benzazepin-2-oneHCID 10017219—
Reactant3-(3,4-Dimethoxyphenylthio)-propylchlorideHCID 20240147—
SolventPyridineHCID 1049—
ProductN-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-[3-(3,4-dimethoxyphenylthio)propyl]-methylamineHCID 13579668—

Reaction Steps

The title compound is prepared from N-[3-(7,8-dimethoxy-1,3,4,5- tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-methylamine and 3-(3,4-dimethoxyphenylthio)-propylchloride with the addition of pyridine analogously to Example 3.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04604389
Source datasetuspto-grants-1986_08
ORD IDord-415027b93e0c453593b58823bfb04e89
Source noteuspto-grants-1986_08