Hydrogen Peroxide → N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(2-phenylsulfinylethyl)-methylamine

HRID 364079Notes

Reaction equation

HRID 364079 reaction equation
[CH3:1][O:2][C:3]1[C:28]([O:29][CH3:30])=[CH:27][C:6]2[CH2:7][C:8](=[O:26])[N:9]([CH2:12][CH2:13][CH2:14][N:15]([CH3:25])[CH2:16][CH2:17][S:18][C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH2:10][CH2:11][C:5]=2[CH:4]=1.[OH:31]O>>[CH3:1][O:2][C:3]1[C:28]([O:29][CH3:30])=[CH:27][C:6]2[CH2:7][C:8](=[O:26])[N:9]([CH2:12][CH2:13][CH2:14][N:15]([CH3:25])[CH2:16][CH2:17][S:18]([C:19]3[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=3)=[O:31])[CH2:10][CH2:11][C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 784Hydrogen PeroxideHCID 13579670N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(2-phenylthioethyl)-methylamine

Product 1

HCID 20240072N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(2-phenylsulfinylethyl)-methylamine

Procedure

The title compound is prepared from N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(2-phenylthioethyl)-methylamine and hydrogen peroxide analogously to Example 4.

Sources & evidence

ORD record
ord-c3fcd9b50f874d9faafe2e6e98425d7a
Source dataset
uspto-grants-1986_08
Patent number
US04604389

Reaction notes

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