Hydrogen Peroxide → HCID 20240071, compound

HRID 364081Notes

Reaction equation

HRID 364081 reaction equation
[CH3:1][O:2][C:3]1[C:32]([O:33][CH3:34])=[CH:31][C:6]2[CH2:7][C:8](=[O:30])[N:9]([CH2:12][CH2:13][CH2:14][N:15]([CH3:29])[CH2:16][CH2:17][S:18][C:19]3[CH:24]=[CH:23][C:22]([O:25][CH3:26])=[C:21]([O:27][CH3:28])[CH:20]=3)[CH2:10][CH2:11][C:5]=2[CH:4]=1.[OH:35]O>>[CH3:1][O:2][C:3]1[C:32]([O:33][CH3:34])=[CH:31][C:6]2[CH2:7][C:8](=[O:30])[N:9]([CH2:12][CH2:13][CH2:14][N:15]([CH3:29])[CH2:16][CH2:17][S:18]([C:19]3[CH:24]=[CH:23][C:22]([O:25][CH3:26])=[C:21]([O:27][CH3:28])[CH:20]=3)=[O:35])[CH2:10][CH2:11][C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 784Hydrogen PeroxideHCID 20240129HCID 20240129, compound

Product 1

HCID 20240071HCID 20240071, compound

Procedure

The title compound is prepared from N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-[2-(3,4-dimethoxyphenylthio)-ethyl]-methylamine and hydrogen peroxide analogously to Example 4.

Sources & evidence

ORD record
ord-242eead726f54f8dbfc3f1bed665afa4
Source dataset
uspto-grants-1986_08
Patent number
US04604389

Reaction notes

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