Hydrogen Peroxide → HCID 20240098, compound

HRID 364085Notes

Reaction equation

HRID 364085 reaction equation
[CH3:1][O:2][C:3]1[C:32]([O:33][CH3:34])=[CH:31][C:6]2[CH2:7][C:8](=[O:30])[N:9]([CH2:12][CH2:13][CH2:14][N:15]([CH3:29])[CH2:16][CH2:17][CH2:18][S:19][C:20]3[CH:25]=[C:24]([Br:26])[C:23]([NH2:27])=[C:22]([Br:28])[CH:21]=3)[CH2:10][CH2:11][C:5]=2[CH:4]=1.[OH:35]O>C(O)(=O)C>[CH3:1][O:2][C:3]1[C:32]([O:33][CH3:34])=[CH:31][C:6]2[CH2:7][C:8](=[O:30])[N:9]([CH2:12][CH2:13][CH2:14][N:15]([CH3:29])[CH2:16][CH2:17][CH2:18][S:19]([C:20]3[CH:25]=[C:24]([Br:26])[C:23]([NH2:27])=[C:22]([Br:28])[CH:21]=3)=[O:35])[CH2:10][CH2:11][C:5]=2[CH:4]=1

Participants

4

Reactant 2

HCID 784Hydrogen PeroxideHCID 70494389HCID 70494389, compound

Product 1

HCID 20240098HCID 20240098, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

The title compound is prepared from N-[3-(7,8-dimethoxy-1,3,4,5-tetra-hydro-2H-3-benzazepin-2-on-3-yl)-propyl-N-[3-(4-amino-3,5-dibromophenylthio)-propyl]-methylamine and hydrogen peroxide in glacial acetic acid analogously to Example 4.

Sources & evidence

ORD record
ord-e7ce1ca5be784736a4109eb0498c194f
Source dataset
uspto-grants-1986_08
Patent number
US04604389

Reaction notes

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