1,1'-Carbonyldiimidazole → HCID 20240074, compound

HRID 364100Notes

Reaction equation

HRID 364100 reaction equation
[NH2:1][C:2]1[CH:7]=[C:6]([O:8][CH3:9])[C:5]([O:10][CH3:11])=[CH:4][C:3]=1[CH2:12][CH2:13][NH:14][CH2:15][CH2:16][CH2:17][N:18]([CH3:29])[CH2:19][CH2:20][CH2:21][S:22][C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1.[C:30](N1C=CN=C1)(N1C=CN=C1)=[O:31]>C(#N)C>[CH3:11][O:10][C:5]1[C:6]([O:8][CH3:9])=[CH:7][C:2]2[NH:1][C:30](=[O:31])[N:14]([CH2:15][CH2:16][CH2:17][N:18]([CH3:29])[CH2:19][CH2:20][CH2:21][S:22][C:23]3[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=3)[CH2:13][CH2:12][C:3]=2[CH:4]=1

Participants

4

Reactant 2

HCID 682631,1'-CarbonyldiimidazoleHCID 20240070HCID 20240070, compound

Product 1

HCID 20240074HCID 20240074, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

The title compound is prepared from N-[3-(2-(2-amino-4,5-dimethoxyphenyl)-ethylamino)-propyl]-N-[3-(phenylthio)-propyl]-methylamine and carbonyldiimidazole in acetonitrile analogously to Example 56.

Sources & evidence

ORD record
ord-f071991bb32e4416b90ca63dddb17688
Source dataset
uspto-grants-1986_08
Patent number
US04604389

Reaction notes

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