Selenium Dioxide → HCID 20240089, compound

HRID 364108Notes

Reaction equation

HRID 364108 reaction equation
[CH3:1][O:2][C:3]1[C:35]([O:36][CH3:37])=[CH:34][C:6]2[CH2:7][C:8](=[O:33])[N:9]([CH2:12][CH2:13][CH2:14][N:15]([CH3:32])[CH2:16][CH2:17][CH2:18][S:19]([C:22]3[CH:27]=[CH:26][C:25]([O:28][CH3:29])=[C:24]([O:30][CH3:31])[CH:23]=3)(=[O:21])=[O:20])[CH2:10][CH2:11][C:5]=2[CH:4]=1.[Se](=O)=[O:39]>>[CH3:1][O:2][C:3]1[C:35]([O:36][CH3:37])=[CH:34][C:6]2[C:7](=[O:39])[C:8](=[O:33])[N:9]([CH2:12][CH2:13][CH2:14][N:15]([CH3:32])[CH2:16][CH2:17][CH2:18][S:19]([C:22]3[CH:27]=[CH:26][C:25]([O:28][CH3:29])=[C:24]([O:30][CH3:31])[CH:23]=3)(=[O:21])=[O:20])[CH2:10][CH2:11][C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 24007Selenium DioxideHCID 20240075HCID 20240075, compound

Product 1

HCID 20240089HCID 20240089, compound

Procedure

The title compound is prepared from N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-[3-(3,4-dimethoxy-phenylsulfonyl)-propyl]-methylamine and selenium dioxide analogously to Example 55.

Sources & evidence

ORD record
ord-64c272fc296b412c9c89a79cbfc03558
Source dataset
uspto-grants-1986_08
Patent number
US04604389

Reaction notes

Loading…