1,1'-Carbonyldiimidazole → HCID 20240113, compound

HRID 364115Notes

Reaction equation

HRID 364115 reaction equation
[NH2:1][C:2]1[CH:7]=[C:6]2[O:8][CH2:9][O:10][C:5]2=[CH:4][C:3]=1[CH2:11][CH2:12][NH:13][CH2:14][CH2:15][CH2:16][N:17]([CH3:32])[CH2:18][CH2:19][CH2:20][S:21][C:22]1[CH:27]=[CH:26][C:25]([O:28][CH3:29])=[C:24]([O:30][CH3:31])[CH:23]=1.[C:33](N1C=CN=C1)(N1C=CN=C1)=[O:34]>C(#N)C>[CH2:9]1[O:8][C:6]2=[CH:7][C:2]3[NH:1][C:33](=[O:34])[N:13]([CH2:14][CH2:15][CH2:16][N:17]([CH3:32])[CH2:18][CH2:19][CH2:20][S:21][C:22]4[CH:27]=[CH:26][C:25]([O:28][CH3:29])=[C:24]([O:30][CH3:31])[CH:23]=4)[CH2:12][CH2:11][C:3]=3[CH:4]=[C:5]2[O:10]1

Participants

4

Reactant 2

HCID 682631,1'-CarbonyldiimidazoleHCID 20240065HCID 20240065, compound

Product 1

HCID 20240113HCID 20240113, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

The title compound is prepared from N-[3-(2-(2-amino-4,5-methylenedioxy-phenyl)-ethylamino)-propyl]-N-[3-(3,4-dimethoxyphenylthio)-propyl]-methylamine and carbonyldiimidazole in acetonitrile analogously to Example 56.

Sources & evidence

ORD record
ord-7b01f453f2d949eeb3b332124db79971
Source dataset
uspto-grants-1986_08
Patent number
US04604389

Reaction notes

Loading…