1,1'-Carbonyldiimidazole → HCID 20240131, compound

HRID 364119Notes

Reaction equation

HRID 364119 reaction equation
[NH2:1][C:2]1[CH:7]=[C:6]([O:8][CH3:9])[C:5]([O:10][CH3:11])=[CH:4][C:3]=1[CH2:12][CH2:13][NH:14][CH2:15][CH2:16][CH2:17][N:18]([CH3:33])[CH2:19][CH2:20][N:21]([C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[C:25]([O:31][CH3:32])[CH:24]=1)[CH3:22].[C:34](N1C=CN=C1)(N1C=CN=C1)=[O:35]>>[CH3:11][O:10][C:5]1[C:6]([O:8][CH3:9])=[CH:7][C:2]2[NH:1][C:34](=[O:35])[N:14]([CH2:15][CH2:16][CH2:17][N:18]([CH3:33])[CH2:19][CH2:20][N:21]([C:23]3[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[C:25]([O:31][CH3:32])[CH:24]=3)[CH3:22])[CH2:13][CH2:12][C:3]=2[CH:4]=1

Participants

3

Reactant 2

HCID 682631,1'-CarbonyldiimidazoleHCID 20240091HCID 20240091, compound

Product 1

HCID 20240131HCID 20240131, compound

Procedure

The title compound is prepared from N-[3-(2-(2-amino-4,5-dimethoxyphenyl)-ethylamino)-propyl]-N-[2-(N-methyl-3,4-dimethoxy-phenylamino)-ethyl]-methylamine and carbonyldiimidazole analogously to Example 56.

Sources & evidence

ORD record
ord-562f31c705dd48aeb65e4e29128f16e6
Source dataset
uspto-grants-1986_08
Patent number
US04604389

Reaction notes

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