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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 364153Generated: October 30, 2026

Cyclohexylamine → HCID 178440548, compound

https://huagongshe.com/reaction/364153

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCyclohexylamineHCID 7965—
ReactantHCID 53956536HCID 53956536—
ProductHCID 178440548HCID 17844054858.2%

Reaction Conditions

Temperature135 °C

Reaction Steps

A mixture of 20 g of allylmethylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride and 9.09 g of cyclohexylamine is heated at 135° C. for 3 hours, and the product is then distilled in vacuo. 16 g of a yellow, viscous oil distill over between 128° and 138° C. at 2.5 Pa, corresponding to a yield of 58.2%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04604437
Source datasetuspto-grants-1986_08
ORD IDord-efa4c0726d064f5f9cfcab91a3c2bed8
Source noteuspto-grants-1986_08