Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 3-Phenylprop-2-Enal | HCID 307 | — |
| Reactant | 2,2-Dimethyl-1,3-dioxane-4,6-dione | HCID 16249 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 576164 | HCID 576164 | — |
Reaction Steps
7.2 g (0.05 mol) of Meldrum's acid and 6.6 g (6.3 ml, 0.05 mol) of cinnamaldehyde were weighed in to 50 ml of the mixture of formic acid and triethylamine prepared as described in Example 1. The reaction mixture was heated to 95° C. during 1 hour and maintained at the same temperature for 2 hours. The product was separated according to Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05414108 |
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| Source dataset | uspto-grants-1995_05 |
|---|
| ORD ID | ord-7ed3b08e75fa49089858a61a38270641 |
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| Source note | uspto-grants-1995_05 |
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