Formic Acid → HCID 576164, compound

HRID 36416Notes

Reaction equation

HRID 36416 reaction equation
CC1(C)[O:9][C:7](=[O:8])[CH2:6][C:4](=O)O1.C(=O)[CH:12]=[CH:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.C(O)=O>C(N(CC)CC)C>[C:14]1([CH:13]=[CH:12][CH2:4][CH2:6][C:7]([OH:9])=[O:8])[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

5

Reactant 3

HCID 284Formic AcidHCID 3073-Phenylprop-2-EnalHCID 162492,2-Dimethyl-1,3-dioxane-4,6-dione

Product 1

HCID 576164HCID 576164, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Conditions

Temperature
95 °C

Procedure

7.2 g (0.05 mol) of Meldrum's acid and 6.6 g (6.3 ml, 0.05 mol) of cinnamaldehyde were weighed in to 50 ml of the mixture of formic acid and triethylamine prepared as described in Example 1. The reaction mixture was heated to 95° C. during 1 hour and maintained at the same temperature for 2 hours. The product was separated according to Example 1.

Workup

  1. customprepared
  2. temperaturemaintained at the same temperature for 2 hours
  3. customThe product was separated

Sources & evidence

ORD record
ord-7ed3b08e75fa49089858a61a38270641
Source dataset
uspto-grants-1995_05
Patent number
US05414108

Reaction notes

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