HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 131714804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 2-[(2-Hydrazinylethyl)amino]ethan-1-ol | HCID 13413808 | — |
| Reactant | 1-Chloro-4-nitro-9H-xanthen-9-one | HCID 13689006 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131714804 | HCID 131714804 | — |
Reaction Steps
A suspension of 2.76 g of 1-chloro-4-nitro-9H-xanthen-9-one, 30 ml of THF, 15 ml of methanol and 1.40 g of 2-[(hydrazinoethyl)amino]-ethanol was stirred at room temperature for three days. The precipitate was collected, washed with THF and dried, providing the title compound, mp 262°-64° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04604390 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-b2a2e186eea043ae91c9071fab630ca1 |
| Source note | uspto-grants-1986_08 |