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HRID364164

反应详情

EQUATION

反应方程式

HRID 364164 的结构方程式

REACTANTS

反应物

3
结构：C1CCOC1
HCID8028

Tetrahydrofuran

C4H8O

结构：NNCCNCCO
HCID13413808

2-[(2-Hydrazinylethyl)amino]ethan-1-ol

C4H13N3O

结构：O=c1c2ccccc2oc2c([N+](=O)[O-])ccc(Cl)c12
HCID13689006

1-Chloro-4-nitro-9H-xanthen-9-one

C13H6ClNO4

PRODUCTS

生成物

1
结构：Cl.O=[N+]([O-])c1ccc2c3c(nn2CCNCCO)-c2ccccc2Oc13
HCID131714804

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

A suspension of 2.76 g of 1-chloro-4-nitro-9H-xanthen-9-one, 30 ml of THF, 15 ml of methanol and 1.40 g of 2-[(hydrazinoethyl)amino]-ethanol was stirred at room temperature for three days. The precipitate was collected, washed with THF and dried, providing the title compound, mp 262°-64° C. (decomp.).

WORKUP

后处理

  1. customThe precipitate was collected
  2. washwashed with THF
  3. customdried