HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-BROMOETHYLAMINE HYDROCHLORIDE → HCID 54585665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-BROMOETHYLAMINE HYDROCHLORIDE | HCID 12208620 | — |
| Reactant | HCID 13689033 | HCID 13689033 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54585665 | HCID 54585665 | 37.5% |
Reaction Steps
A solution of 5.0 g (0.015 mol) of 5-amino-N,N-diethyl-2H[1]benzothiopyrano[4,3,2-cd]indazole-2-ethanamine and 9.2 g (0.045 mol) of 2-bromoethylamine, hydrochloride in 50 ml of EtOH was heated under reflux for four days and allowed to cool to room temperature. The solid was collected and recrystallized from MeOH to give 2.6 g of product, mp 263° C. dec.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04604390 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-2ff49878ebf94ee5baacf63be9912c73 |
| Source note | uspto-grants-1986_08 |