Hydrogen Bromide → HCID 20240170, compound

HRID 364200Notes

Reaction equation

[NH2:1][C:2]1[CH:10]=[CH:9][C:8]2[N:7]([CH2:11][CH2:12][N:13]([CH2:16][CH3:17])[CH2:14][CH3:15])[N:6]=[C:5]3[C:18]4[CH:24]=[CH:23][CH:22]=[C:21]([O:25]C)[C:19]=4[S:20][C:3]=1[C:4]=23.Br>>[NH2:1][C:2]1[CH:10]=[CH:9][C:8]2[N:7]([CH2:11][CH2:12][N:13]([CH2:16][CH3:17])[CH2:14][CH3:15])[N:6]=[C:5]3[C:18]4[CH:24]=[CH:23][CH:22]=[C:21]([OH:25])[C:19]=4[S:20][C:3]=1[C:4]=23

Participants

Reactant 2

HCID 260Hydrogen Bromide

HCID 20240197HCID 20240197, compound

Product 1

HCID 20240170HCID 20240170, compound

Procedure

Reaction of 5-amino-N,N-diethyl-7-methoxy-2H[1]benzothiopyrano[4,3,2-cd]indazole-2-ethanamine with 48% HBr as described in Example 64 gave the product.

Workup

customgave the product

Sources & evidence

ORD record: ord-d07ab53330194b46aed7a8060d9e4445
Source dataset: uspto-grants-1986_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04604390

Reaction notes

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