Hydrogen Bromide → HCID 178464042, compound

HRID 364202Notes

Reaction equation

HRID 364202 reaction equation
[NH2:1][C:2]1[CH:10]=[CH:9][C:8]2[N:7]([CH2:11][CH2:12][N:13]([CH2:16][CH3:17])[CH2:14][CH3:15])[N:6]=[C:5]3[C:18]4[CH:24]=[CH:23][C:22]([O:25]C)=[CH:21][C:19]=4[S:20][C:3]=1[C:4]=23.Br>>[NH2:1][C:2]1[CH:10]=[CH:9][C:8]2[N:7]([CH2:11][CH2:12][N:13]([CH2:16][CH3:17])[CH2:14][CH3:15])[N:6]=[C:5]3[C:18]4[CH:24]=[CH:23][C:22]([OH:25])=[CH:21][C:19]=4[S:20][C:3]=1[C:4]=23

Participants

3

Reactant 2

HCID 260Hydrogen BromideHCID 144067865-amino-N,N-diethyl-8-methoxy-2H-[1]benzothiopyrano[4,3,2-cd]indazole-2-ethanamine

Product 1

HCID 178464042HCID 178464042, compound

Procedure

Reaction of 5-amino-N,N-diethyl-8-methoxy-2H-[1]benzothiopyrano[4,3,2-cd]indazole-2-ethanamine with 48% HBr as described in Example 64 gave the product.

Workup

  1. customgave the product

Sources & evidence

ORD record
ord-eb76223ec1f34e00a0f656a37981bbdf
Source dataset
uspto-grants-1986_08
Patent number
US04604390

Reaction notes

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