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HRID364203

反应详情

EQUATION

反应方程式

HRID 364203 的结构方程式

REACTANTS

反应物

2
结构：CCN(CC)CCNN
HCID3028735

Ethanamine, N,N-diethyl-2-hydrazino-

C6H17N3

结构：COc1cccc2sc3c([N+](=O)[O-])ccc(Cl)c3c(=O)c12
HCID20240208

未命名化合物

PRODUCTS

生成物

1
结构：CCN(CC)CCn1nc2c3c(c([N+](=O)[O-])ccc31)Sc1cccc(OC)c1-2
HCID20240173

未命名化合物

收率 51.7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Reaction of a mixture of 2.5 g (0.0192 mol) of 2-(diethylaminoethyl)hydrazine, 4.2 g (0.0131 mol) of 1-chloro-8-methoxy-4-nitro-9H-thioxanthen-9-one in 110 ml of DMF as described in Example 53 gave 2.7 g of product.