Ethanamine, N,N-diethyl-2-hydrazino- → HCID 20240173, compound

HRID 364203Notes

Reaction equation

HRID 364203 reaction equation
[CH2:1]([N:3]([CH2:6][CH2:7][NH:8][NH2:9])[CH2:4][CH3:5])[CH3:2].Cl[C:11]1[C:24]2[C:23](=O)[C:22]3[C:17](=[CH:18][CH:19]=[CH:20][C:21]=3[O:26][CH3:27])[S:16][C:15]=2[C:14]([N+:28]([O-:30])=[O:29])=[CH:13][CH:12]=1>CN(C=O)C>[CH2:1]([N:3]([CH2:4][CH3:5])[CH2:6][CH2:7][N:8]1[C:11]2[CH:12]=[CH:13][C:14]([N+:28]([O-:30])=[O:29])=[C:15]3[S:16][C:17]4[CH:18]=[CH:19][CH:20]=[C:21]([O:26][CH3:27])[C:22]=4[C:23]([C:24]=23)=[N:9]1)[CH3:2]

Participants

4

Reactant 2

HCID 3028735Ethanamine, N,N-diethyl-2-hydrazino-HCID 20240208HCID 20240208, compound

Product 1

HCID 20240173HCID 20240173, compoundYield 51.7%

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Reaction of a mixture of 2.5 g (0.0192 mol) of 2-(diethylaminoethyl)hydrazine, 4.2 g (0.0131 mol) of 1-chloro-8-methoxy-4-nitro-9H-thioxanthen-9-one in 110 ml of DMF as described in Example 53 gave 2.7 g of product.

Sources & evidence

ORD record
ord-c0ecf234320b4815adc544f57aad93f9
Source dataset
uspto-grants-1986_08
Patent number
US04604390

Reaction notes

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