Hydrogen Bromide → HCID 20240220, compound

HRID 364206Notes

Reaction equation

HRID 364206 reaction equation
[NH2:1][C:2]1[CH:10]=[C:9]([O:11]C)[C:8]2[N:7]([CH2:13][CH2:14][N:15]([CH2:18][CH3:19])[CH2:16][CH3:17])[N:6]=[C:5]3[C:20]4[CH:26]=[CH:25][CH:24]=[CH:23][C:21]=4[S:22][C:3]=1[C:4]=23.Br>>[NH2:1][C:2]1[C:3]2[S:22][C:21]3[CH:23]=[CH:24][CH:25]=[CH:26][C:20]=3[C:5]3=[N:6][N:7]([CH2:13][CH2:14][N:15]([CH2:16][CH3:17])[CH2:18][CH3:19])[C:8](=[C:9]([OH:11])[CH:10]=1)[C:4]=23

Participants

3

Reactant 2

HCID 260Hydrogen BromideHCID 20240186HCID 20240186, compound

Product 1

HCID 20240220HCID 20240220, compound

Procedure

Reaction of 5-amino-N,N-diethyl-3-methoxy-2H[1]benzothiopyrano[4,3,2-cd]indazole-2-ethanamine with 48% HBr as described in Example 64 gave the product.

Workup

  1. customgave the product

Sources & evidence

ORD record
ord-d732b1933d9a43e2b9b534753c50e65c
Source dataset
uspto-grants-1986_08
Patent number
US04604390

Reaction notes

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