Hydrogen Bromide → HCID 20240227, compound

HRID 364208Notes

Reaction equation

[NH2:1][C:2]1[CH:10]=[C:9]([O:11]C)[C:8]2[N:7]([CH2:13][CH2:14][N:15]([CH2:18][CH3:19])[CH2:16][CH3:17])[N:6]=[C:5]3[C:20]4[CH:26]=[C:25]([O:27]C)[CH:24]=[CH:23][C:21]=4[S:22][C:3]=1[C:4]=23.Br>>[NH2:1][C:2]1[C:3]2[S:22][C:21]3[CH:23]=[CH:24][C:25]([OH:27])=[CH:26][C:20]=3[C:5]3=[N:6][N:7]([CH2:13][CH2:14][N:15]([CH2:18][CH3:19])[CH2:16][CH3:17])[C:8](=[C:9]([OH:11])[CH:10]=1)[C:4]=23

Participants

Reactant 2

HCID 260Hydrogen Bromide

HCID 20240182HCID 20240182, compound

Product 1

HCID 20240227HCID 20240227, compound

Procedure

Reaction of 5-amino-N,N-diethyl-3,9-dimethoxy-2H[1]benzothiopyrano[4,3,2-cd]indazole-2-ethanamine with 48% HBr as described in Example 64 gave the product.

Workup

customgave the product

Sources & evidence

ORD record: ord-12eb72b77fd24738badb9d4f917da984
Source dataset: uspto-grants-1986_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04604390

Reaction notes

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