HRID364421

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID674

Dimethylamine

C2H7N

HCID971

Oxalic acid

C2H2O4

HCID13729322

未命名化合物

2 次

PRODUCTS

生成物

结构：CN(C)CC1CN(C2CCCCC2)C(=O)c2cccnc2O1.O=C(O)C(=O)O

HCID21271464

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

Utilizing the procedure of Example 10, 2-(chloromethyl)-4-cyclohexyl-2,3-dihydropyrido[3,2-f][1,4]oxazepin-5(4H)-one (Intermediate 35) is reacted with 40% aqueous dimethylamine and reacted with oxalic acid in isopropyl alcohol.