Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 36446Generated: October 30, 2026

HCID 19938135, compound → N-{2-[Bis(4-hydroxyphenyl)methyl]phenyl}-4-aminobenzamide

https://huagongshe.com/reaction/36446

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19938135HCID 19938135—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductN-{2-[Bis(4-hydroxyphenyl)methyl]phenyl}-4-aminobenzamideHCID 1993809638.4%

Reaction Steps

In 50 ml of methanol were suspended 1.48 g of Compound 117 obtained by Example 117 and 0.23 g of 10% palladium-carbon, and the suspension was stirred under hydrogen atmosphere at room temperature for 2 hours. After the reaction was completed, the reaction mixture was filtered by using a filter aid. The solvent was evaporated under reduced pressure to afford 0.53 g of the desired compound (Compound 136).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05413997
Source datasetuspto-grants-1995_05
ORD IDord-83c9c889211b4610b50da3a3d18c1597
Source noteuspto-grants-1995_05