HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19938135, compound → N-{2-[Bis(4-hydroxyphenyl)methyl]phenyl}-4-aminobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19938135 | HCID 19938135 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-{2-[Bis(4-hydroxyphenyl)methyl]phenyl}-4-aminobenzamide | HCID 19938096 | 38.4% |
Reaction Steps
In 50 ml of methanol were suspended 1.48 g of Compound 117 obtained by Example 117 and 0.23 g of 10% palladium-carbon, and the suspension was stirred under hydrogen atmosphere at room temperature for 2 hours. After the reaction was completed, the reaction mixture was filtered by using a filter aid. The solvent was evaporated under reduced pressure to afford 0.53 g of the desired compound (Compound 136).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05413997 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-83c9c889211b4610b50da3a3d18c1597 |
| Source note | uspto-grants-1995_05 |