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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 36447Generated: October 30, 2026

HCID 19938212, compound → HCID 19938195, compound

https://huagongshe.com/reaction/36447

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19938212HCID 19938212—
SolventHydrochloric AcidHCID 313—
SolventEthyl AcetateHCID 8857—
ProductHCID 19938195HCID 1993819517.2%

Reaction Steps

In 50 ml of ethyl acetate saturated with hydrogen chloride was dissolved 2.18 g of Compound 137 obtained by Example 137, and the solution was stirred for 1 hour. Thereafter, the solvent was evaporated under reduced pressure, and the residue was recrystallized from methanol to afford 0.31 g of the desired compound (Compound 138).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05413997
Source datasetuspto-grants-1995_05
ORD IDord-6cc0d8f109b1402ab5ccb3f8e17ba093
Source noteuspto-grants-1995_05