HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19938212, compound → HCID 19938195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19938212 | HCID 19938212 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 19938195 | HCID 19938195 | 17.2% |
Reaction Steps
In 50 ml of ethyl acetate saturated with hydrogen chloride was dissolved 2.18 g of Compound 137 obtained by Example 137, and the solution was stirred for 1 hour. Thereafter, the solvent was evaporated under reduced pressure, and the residue was recrystallized from methanol to afford 0.31 g of the desired compound (Compound 138).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05413997 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-6cc0d8f109b1402ab5ccb3f8e17ba093 |
| Source note | uspto-grants-1995_05 |