HRID36447

反应详情

EQUATION

反应方程式

HRID 36447 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

In 50 ml of ethyl acetate saturated with hydrogen chloride was dissolved 2.18 g of Compound 137 obtained by Example 137, and the solution was stirred for 1 hour. Thereafter, the solvent was evaporated under reduced pressure, and the residue was recrystallized from methanol to afford 0.31 g of the desired compound (Compound 138).

WORKUP

后处理

  1. customThereafter, the solvent was evaporated under reduced pressure
  2. customthe residue was recrystallized from methanol