HRID36451

反应详情

EQUATION

反应方程式

HRID 36451 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

By a procedure analogous to that of Example 1, but using 1.96 g of ethyl diethoxymethylphosphinate and 20 ml of a molar solution of benzylmagnesium chloride in diethyl ether and adding 4.14 g of potassium carbonate in 5 ml of water to precipitate inorganic salts, benzyl(diethoxymethyl)phosphine oxide is obtained as a colourless oil.

WORKUP

后处理

  1. customto precipitate inorganic salts