Potassium Carbonate → HCID 178468026, compound

HRID 36453Notes

Reaction equation

HRID 36453 reaction equation
[CH2:1]([O:3][C:4]([PH:9](=[O:13])OCC)([O:6][CH2:7][CH3:8])[CH3:5])[CH3:2].[CH3:14][Mg]Cl.C(=O)([O-])[O-].[K+].[K+]>O>[CH3:14][PH:9](=[O:13])[C:4]([O:6][CH2:7][CH3:8])([O:3][CH2:1][CH3:2])[CH3:5]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 178418332HCID 178418332, compoundHCID 178476820HCID 178476820, compound

Product 1

HCID 178468026HCID 178468026, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

By a procedure analogous to that of Example 1, but using ethyl 1,1-diethoxyethylphosphinate (10.5 g) and 33.5 ml of the methylmagnesium chloride solution and adding 14.1 g of potassium carbonate in 30 ml of water to precipitate inorganic salts, methyl (1,1-diethoxyethyl)phosphine oxide is obtained as a colourless oil.

Workup

  1. customto precipitate inorganic salts

Sources & evidence

ORD record
ord-0ce1a03dac0541488a556df9fb9a45e8
Source dataset
uspto-grants-1995_05
Patent number
US05414133

Reaction notes

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