Hydrochloric Acid → HCID 178454899, compound

HRID 36458Notes

Reaction equation

HRID 36458 reaction equation
[C:1]([P:5](=[O:20])([CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)C(OCC)OCC)([CH3:4])([CH3:3])[CH3:2].Cl>>[C:1]([PH:5](=[O:20])[CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 19938721Tert.butyl(benzyl)(diethoxymethyl)phosphine oxide

Product 1

HCID 178454899HCID 178454899, compound

Procedure

Following a procedure analogous to that to Example 13, but using tert.butyl(benzyl)(diethoxymethyl)phosphine oxide (1.7 g) and 15 ml of concentrated hydrochloric acid, tert.butyl(benzyl)phosphine oxide is obtained as a white solid, m.p. 80°-2° C.

Sources & evidence

ORD record
ord-11c9391b17f14c5caca7af0c8580618c
Source dataset
uspto-grants-1995_05
Patent number
US05414133

Reaction notes

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