Ammonium Hydroxide → HCID 86740959, compound

HRID 364858Notes

Reaction equation

HRID 364858 reaction equation
[Na].[CH:2]1([CH3:15])[CH2:7][CH2:6][CH:5]([CH:8]([CH3:10])[CH3:9])[CH2:4][CH:3]1[S:11]([O-:14])(=[O:13])=[O:12].C1(C)CCC(C(C)C)CC1S(O)(=O)=O.[OH-].[NH4+:31]>>[CH:2]1([CH3:15])[CH2:7][CH2:6][CH:5]([CH:8]([CH3:10])[CH3:9])[CH2:4][CH:3]1[S:11]([O-:14])(=[O:13])=[O:12].[NH4+:31]

Participants

4

Reactant 3

HCID 14923Ammonium HydroxideHCID 20238455HCID 20238455, compoundHCID 86740960HCID 86740960, compound

Product 1

HCID 86740959HCID 86740959, compound

Procedure

Sodium-p-menthane-2-sulfonate, 35 grams, prepared as in Example 9 was passed through an ion-exchange column. The eluate containing p-menthane-2-sulfonic acid was neutralized with dilute ammonium hydroxide. The solution was evaporated to dryness and the residue stored in vacuo over phosphorus pentoxide. The product was 91.7% pure by NMR analysis.

Workup

  1. customThe solution was evaporated to dryness

Sources & evidence

ORD record
ord-36a6a5654fc541b1be986e91a2aab65c
Source dataset
uspto-grants-1986_08
Patent number
US04606851

Reaction notes

Loading…