HRID364874

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].[Al+3].[Al+3]

HCID24850

Aluminum Sulfate

Al2O12S3

结构：CCCCCCCCCCCCCC(=O)N[C@@H](CCC(=O)[O-])C(=O)[O-].[Na+].[Na+]

HCID71587140

Disodium myristoyl glutamate

C19H33NNa2O5

PRODUCTS

生成物

结构：CCCCCCCCCCCCCC(=O)N[C@@H](CCC(=O)[O-])C(=O)[O-].CCCCCCCCCCCCCC(=O)N[C@@H](CCC(=O)[O-])C(=O)[O-].CCCCCCCCCCCCCC(=O)N[C@@H](CCC(=O)[O-])C(=O)[O-].[Al+3].[Al+3]

HCID56843224

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID962

Water

H2O

PROCEDURE

实验过程

Sodium N-myristoyl-L-glutamate was added to a suspension in which 30 g of sericite had been suspended in 4 liters of water. Then, stirring was fully carried out. Into this suspension was added 60 ml of a 20% aqueous solution of aluminum sulfate in 10 minutes. Then, further stirring was carried out for 10 minutes. Thereafter, the suspension was dehydrated by means of a basket type centrifuge. Then, drying was carried out at 110° C. in a hot-air drying apparatus to produce about 1 kg of a dried product. The dried product thus obtained was crushed by means of a high-speed mixer (hexyl mixer) to a light degree.

WORKUP

后处理

stirringThen, further stirring
customThen, drying
customwas carried out at 110° C. in a hot-air drying apparatus

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-e1103b5d5638410bade466667e08a029
来源数据集: uspto-grants-1986_08
DOI: 10.6084/m9.figshare.5104873.v1
专利: US04606914
来源说明: uspto-grants-1986_08

反应 SMILES

[C:1]([NH:16][C@H:17]([C:23]([O-:25])=[O:24])[CH2:18][CH2:19][C:20]([O-:22])=[O:21])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Na+].[Na+].S([O-])([O-])(=O)=O.[Al+3:33].S([O-])([O-])(=O)=O.S([O-])([O-])(=O)=O.[Al+3]>O>[C:1]([NH:16][C@H:17]([C:23]([O-:25])=[O:24])[CH2:18][CH2:19][C:20]([O-:22])=[O:21])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Al+3:33].[C:1]([NH:16][C@H:17]([C:23]([O-:25])=[O:24])[CH2:18][CH2:19][C:20]([O-:22])=[O:21])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[C:1]([NH:16][C@H:17]([C:23]([O-:25])=[O:24])[CH2:18][CH2:19][C:20]([O-:22])=[O:21])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Al+3:33]