HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → HCID 13765211, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 13765210 | HCID 13765210 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13765211 | HCID 13765211 | — |
Reaction Steps
A mixture composed of 93.0 g of (1-c), 22.3 g of p-toluenesulfonic acid monohydrate and 1 l of toluene was refluxed with heating for 3 hours to distill away the water formed. After being allowed to cool, the crystals formed were washed with acetone and dried. Yield: 73 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04606991 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-f252c38707b144f3a93af4b46ebbbceb |
| Source note | uspto-grants-1986_08 |