Lawesson's reagent → HCID 13712238, compound

Participants

Reaction Steps

36.7 g of 4-methyl-2',5'-difluorobenzanilide was dissolved in 170 ml of toluene, and 36 g of Lawesson's reagent was added. The mixture was refluxed for 1 hour. The reaction mixture was evaporated to dryness under reduced pressure. The residue was recrystallized from 100 ml of benzene to give 35.0 g of the captioned compound as yellow needle-like crystals.

Provenance & Evidence