HCID 70040791, compound → HCID 70455662, compound

Participants

Reaction Steps

4-(1-Imidazolylmethyl)cinnamic acid hydrochloride is dissolved by heating in an adequate amount of 50% (V/V%) aqueous acetone and filtrated and the filtrate is diluted with acetone in an amount sufficient to make an aqueous solution of acetone having water content of about 10-30% (V/V%), preferably about 17% (V/V%). The mixture is allowed to stand at room temperature for an adequate period of time. The precipitates are collected and dried under reduced pressure at room temperature to obtain 4-(1-imidazolylmethyl)cinnamic acid hydrochloride monohydrate.

Provenance & Evidence