Acetone → HCID 70455662, compound

Participants

Reaction Steps

In 60 ml of aqueous solution of acetone having water content of 25% (V/V%), 10 g of 4-(1-imidazolylmethyl)cinnamic acid hydrochloride was dissolved by heating and then the solution was allowed to stand overnight at room temperature. The resulting precipitates were collected by filtration and dried at room temperature for 3 hr under reduced pressure to obtain 7.0 g of 4-(1-imidazolylmethyl)cinnamic acid hydrochloride monohydrate. This product had the same IR-absorption spectrum and NMR spectrum as those of the product of EXAMPLE 1.

Provenance & Evidence