HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylamine → 3-[[4-(1-Hexenyl)benzoyl]ethoxyamino]pentanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylamine | HCID 7582 | — |
| Reactant | 1-Bromononane | HCID 12742 | — |
| Reactant | O-ethylhydroxylamine hydrochloride | HCID 76850 | — |
| Reactant | O-Methylhydroxylamine hydrochloride | HCID 521874 | — |
| Reactant | Ethyl 4-iodobutanoate | HCID 10890062 | — |
| Reactant | Ethyl-3 iodovalerate | HCID 20238940 | — |
| Product | 3-[[4-(1-Hexenyl)benzoyl]ethoxyamino]pentanoic acid | HCID 57061393 | — |
Reaction Steps
Following the procedure of Example 7 except substituting 1-bromopentane for 1-bromononane, ethoxylamine hydrochloride for methoxylamine hydrochloride and ethyl-3 iodovalerate for ethyl-4-iodobutyrate, and eliminating the addition of dicyclohexylamine, the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04607053 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-2ce856bda49f44488af030f641f02af4 |
| Source note | uspto-grants-1986_08 |