HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 13689354, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 13689353 | HCID 13689353 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13689354 | HCID 13689354 | — |
Reaction Steps
To a suspension of sodium hydride (2.0 g, 50% in oil, treated with hexanes, 0.04 mole) in 50 ml benzene was added a suspension of [1-(2-fluorobenzyl)-2-pyrryl]-[(1-methyl)piperidin-4-yl]methanol (10.0 g, 0.033 mole) in 100 ml benzene, followed by 50 ml dimethylformamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04608374 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-3df129a011d24c29826f71199ada4395 |
| Source note | uspto-grants-1986_08 |