HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 20191667, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-(3-Chloropropyl)-6-fluorobenzo[d]isoxazole | HCID 10910880 | — |
| Reactant | HCID 14712340 | HCID 14712340 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20191667 | HCID 20191667 | — |
Reaction Steps
To 50 ml dry DMF were added 11-(piperidin-4-yl)-5H,11H-pyrrolo2,1-c][1,4]benzoxazepine (3.0 g, 0.0112 mole), 3-(3-chloropropyl)-6-fluoro-1,2-benzisoxazole (4.2 g, 0.02 mole), milled K2CO3 (10 g, 0.07 mole) and KI (0.01 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04608374 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-0c183e3d50aa4ffe893db4480b73dc45 |
| Source note | uspto-grants-1986_08 |