HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl Chloride → HCID 13689399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl Chloride | HCID 8005 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 11-(piperdin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine | HCID 13689358 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13689399 | HCID 13689399 | — |
Reaction Steps
A solution of 11-(piperidin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine (6.1 g, 0.023 mole), 1-chlorobutane (2.42 g, 0.026 mole), K2CO3 (10 g) and KI (0.1 g) in 100 ml dimethylformamide was heated at 70° C. for a total of 7 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04608374 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-2b3ee13daf984c449869ae8ff484aa5b |
| Source note | uspto-grants-1986_08 |