HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminophenol → HCID 18316812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminophenol | HCID 11568 | — |
| Reactant | 1-Bromoheptane | HCID 12369 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18316812 | HCID 18316812 | 62% |
Reaction Steps
0.11 mol of n-heptyl bromide and 0.1 mol of NaHCO3 are added to 0.1 mol of m-aminophenol in 150 ml of methanol, and the mixture is refluxed for 5 h. After cooling, it is filtered and the solvent is removed in vacuo. The oil which remains is fractionated in vacuo, to give 3-(n-heptyl-amino)phenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06126867 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-98087601a2ad43deb6466435c9860b43 |
| Source note | uspto-grants-2000_10 |