HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23291342, compound → HCID 23291358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23291342 | HCID 23291342 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23291358 | HCID 23291358 | 62% |
Reaction Steps
A solution of 6-hydroxymethyl-5-(2-methoxymethoxy-4-methoxyphenyl)-4-propoxy-pyrimidine in CH2Cl2 was treated with MnO2 and stirred vigorously for 24 h. The mixture was filtered through celite and concentrated to afford the title compound (1.48 g, 62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06127371 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-b66188b427e747a894c8fb7b5465b345 |
| Source note | uspto-grants-2000_10 |