反应详情

8.4 g of (+/-)-cis-1,2-dimethoxy-4-(2-nitrocyclohex-4-enyl)benzene are dissolved in 450 ml of methanol, treated with 2 ml of conc. hydrochloric acid and hydrogenated after addition of 500 mg of Pd/C 10% strength. The reaction mixture is filtered and the filtrate is concentrated. M.p.: 84-86.5° C.; yield quantitative.

1. filtrationThe reaction mixture is filtered
2. concentrationthe filtrate is concentrated
3. customyield quantitative