Hydrochloric Acid → HCID 178499561, compound

HRID 365442Notes

Reaction equation

HRID 365442 reaction equation
[ClH:1].[NH:2]1[CH:6]=[C:5]([CH2:7][C:8]([OH:10])=[O:9])[N:4]=[CH:3]1.Cl.[CH3:12]O>>[ClH:1].[CH3:12][O:9][C:8](=[O:10])[CH2:7][C:5]1[N:4]=[CH:3][NH:2][CH:6]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 178479752HCID 178479752, compound

Product 1

HCID 178499561HCID 178499561, compound

Procedure

A solution of 1H-imidazole-4-acetic acid hydrochloride (4.00 g, 24.6 mmol) in methanol (100 ml) was saturated with gaseous hydrogen chloride. The resulting solution was allowed to stand at room temperature (RT) for 18 hr. The solvent was evaporated in vacuo to afford the title compound as a white solid.

Workup

  1. customto stand at room temperature
  2. custom(RT)
  3. customfor 18 hr
  4. customThe solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-d94b90aefa89496eaf25d82ce3bb79c8
Source dataset
uspto-grants-2000_10
Patent number
US06127366

Reaction notes

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