HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → HCID 19097440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | Ethyl 6-chloronicotinate | HCID 2799611 | — |
| Product | HCID 19097440 | HCID 19097440 | — |
| Product | 6-(Cyclohexylamino)pyridine-3-carboxylic acid | HCID 23292054 | — |
Reaction Steps
2-Chloro-5-pyridinecarboxylicacid ethylester (g,,5.0 mMol) was treated with 10 mMol cyclohexylamine and the mixture heated for 6 hours at 100° in a sealed tube. Preparative HPLC of the crude product gave the title compound along with equal amounts of the N-cyclohexylamide of the starting ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06127390 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-3d40e028299f4be9b5c1700f8943720b |
| Source note | uspto-grants-2000_10 |