ethyl 2-(3,4-dihydronaphthalen-2-yl)acetate → HCID 54427283, compound

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Reaction Steps

A mixture of 26 g (0.12 mol) of the ester obtained in Step 1 of Example 1 and 2.50 g of Pd/C 10% in 250 ml of EtOH is hydrogenated under 1 bar, at 20° C., overnight. After filtering off the catalyst and washing with ethanol, the filtrate is concentrated in vacuo to yield the expected compound in the form of a colourless oil.

Provenance & Evidence