Ammonium formate → HCID 23292348, compound

Participants

Reaction Steps

0.45 g of ammonium formate is added to a vigorously stirred suspension of 0.35 g (0.84 mmol) of the compound obtained in Step 4 and 0.25 g of Pd/C 10% in 25 ml of CH3OH. After stirring for 1 hour under reflux, the mixture is cooled and filtered; the catalyst is washed with CH3OH and the combined filtrates are concentrated in vacuo to yield the title compound in the form of an oil, which is used without purification in the following reaction.

Provenance & Evidence